检测项目

1.丙烷含量测定:体积分数≥95.0%,偏差允许±0.5%

2.丁烷含量测定:体积分数≥90.0%,杂质烃类≤5.0%

3.总硫含量检测:最大限值50mg/m³,精度要求±0.1mg/m³

4.水分含量分析:水含量≤50mg/kg,采用重量法或卡尔费休法

5.蒸发残留物测定:残留物质量≤10mg/100mL,高温蒸发后称重

6.密度测量:标准密度0.50-0.58g/cm³,温度补偿至15°C

7.蒸气压测试:雷德蒸气压范围100-150kPa,温度37.8°C下测定

8.铜片腐蚀评估:腐蚀等级≤1级,暴露时间2小时at40°C

9.气味强度检测:气味阈值符合安全标准,无刺激性异味

10.烃类组分分布:C3-C4烃类占比≥98%,非烃类杂质≤2%

11.非烃类杂质分析:氧气含量≤0.5%,氮气含量≤1.0%

12.热值计算:净热值≥46MJ/kg,基于组分分析结果

13.挥发性组分检测:轻烃组分如乙烷≤0.1%,避免蒸发损失

14.残留碳质测定:碳质残留≤5mg/kg,高温裂解后分析

15.酸性物质检测:硫化氢含量≤5mg/m³,确保无腐蚀性

检测范围

1.家用液化石油气:用于烹饪和供暖,侧重组分纯度和安全性

2.工业用液化石油气:高温应用,关注热值和杂质控制

3.车用液化石油气:汽车燃料,要求低硫和稳定蒸气压

4.纯丙烷气:丙烷含量≥99.5%,用于特殊工业过程

5.纯丁烷气:丁烷含量≥99.0%,适用于打火机燃料

6.混合液化石油气:丙烷和丁烷混合比例可变,检测组分分布

7.液化石油气添加剂:如odorants,检测添加量和均匀性

8.液化石油气残液:使用后残留物,分析蒸发特性和杂质

9.进口液化石油气:符合国际标准,进行全项目检测

10.出口液化石油气:满足目标市场要求,如低硫限值

11.高纯度液化石油气:用于电子行业,杂质总量≤0.1%

12.低硫液化石油气:总硫≤10mg/m³,环保应用

13.液化石油气样品:实验室小样,进行快速筛查分析

14.液化石油气储罐残留:清理后检测,确保无危险物质

15.特种液化石油气:如医用级,要求极高纯度和无菌性

检测方法

国际标准:

ASTMD2163-23JianCeTestMethodforAnalysisofLiquefiedPetroleum(LP)GasesandPropaneConcentratesbyGasChromatography

ISO8975:2022Liquefiedpetroleumgases—Calculationofvapourpressureandrelativedensity

ASTMD1265-23JianCePracticeforSamplingLiquefiedPetroleum(LP)Gases

ISO4256:2021Liquefiedpetroleumgases—Determinationofgaugevapourpressure

ASTMD2784-23JianCeTestMethodforSulfurinLiquefiedPetroleumGases(Oxy-HydrogenBurnerorLamp)

ISO8819:2022Liquefiedpetroleumgases—Detectionofhydrogensulfide—Leadacetatemethod

ASTMD2713-23JianCeTestMethodforDrynessofPropane(ValveFreezeMethod)

ISO8973:2022Liquefiedpetroleumgases—Calculationofdensityandvapourpressure

ASTMD1838-23JianCeTestMethodforCopperStripCorrosionbyLiquefiedPetroleum(LP)Gases

ISO9162:2021Liquefiedpetroleumgases—Determinationofammonia

ASTMD2158-23JianCeTestMethodforResiduesinLiquefiedPetroleum(LP)Gases

ISO10101-2:2022Naturalgas—Determinationofwatercontent—Part2:KarlFischermethod

国家标准:

GB/T1JianCe1-2021JianCetestmethodforsulfurinpetroleumproductsbywavelengthdispersiveX-rayfluorescencespectrometry

GB/T12576-2021Liquefiedpetroleumgases—Calculationofvapourpressureandrelativedensity

GB/T17623-2021Determinationofcomponentsinliquefiedpetroleumgases—Gaschromatographicmethod

GB/T18619.1-2021Naturalgas—Determinationofwatercontent—Part1:KarlFischermethod

GB/T27867-2021Liquefiedpetroleumgases—Determinationofresidue

GB/T3555-2021Petroleumproducts—Determinationofcorrosionpotential

GB/T11060.1-2021Naturalgas—Determinationofsulfurcompounds—Part1:Hydrogensulfide

GB/T13610-2021Naturalgas—Compositionalanalysisbygaschromatography

GB/T17283-2021Determinationofvapourpressureofpetroleumproducts—Reidmethod

GB/T18619.2-2021Naturalgas—Determinationofwatercontent—Part2:Electronicmoistureanalyzers

GB/T27894.1-2021Naturalgas—Determinationofcompositionwithdefineduncertaintybygaschromatography—Part1:Guidelinesfortailoredanalysis

检测设备

1.气相色谱仪:型号GC-2020.用于烃类组分分析,检测限0.01%,配备FID检测器

2.硫分析仪:型号S-550.采用紫外荧光法,总硫检测范围0.1-100mg/m³,精度±0.05mg/m³

3.水分测定仪:型号M-200.基于卡尔费休法,水分测量范围1-1000mg/kg,分辨率0.1mg/kg

4.自动密度计:型号D-300.振动管原理,密度测量精度±0.0001g/cm³,温度控制±0.1°C

5.蒸气压测定仪:型号VP-400.雷德法标准设备,压力范围0-200kPa,精度±0.5kPa

6.铜片腐蚀测试仪:型号C-500.恒温控制40°C,腐蚀等级评估符合ASTM标准

7.蒸发残留物装置:型号ER-250.高温蒸发系统,残留物称重精度±0.1mg

8.热值计算仪:型号CV-350.基于色谱数据自动计算热值,精度±0.1MJ/kg

9.气体采样系统:型号GS-100.确保样品代表性,压力调节范围0-1MPa

10.痕量杂质分析仪:型号GCMS-2000.气相色谱-质谱联用,检测非烃类杂质下限0.001%